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RSC Adv., 2020, 10, 9736-9744 Permissions. Request permissions A new spinel high-entropy ... 99.9%) and CuO (0.01 mol, 0.7954 g, 99.9%) were mixed as pre-alloyed powder by a planetary ball mill. To ensure adequate mixing, all pre-alloyed powder was milled for at least 2 hours. The mixed powder was then separated into several samples with a ...
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1.0 eq. of the isocyanogold(I) complex and 2.0 eq. of the aniline derivative are transferred to a ball milling vessel (stainless steel, 20 ml) containing 10 grinding balls (stainless steel, diameter: 5 mm). The vessel was then transferred to a ball mill (Pulverisette 7 premium line, Fritsch) and the mixture is milled for a denounced time.
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Spex 8000M mixer mill, stainless steel vial and ball (5 mm), 18 Hz, stainless steel ball (5 mm). Reproduced from Shearouse WC, Korte CM, Mack J. A two-step ball milling method synthesizes and purifies α,β-unsaturated esters. Green Chem 2011;13:598–601, with permission from the Royal Society of Chemistry.
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WO 3 and carbon black were mixed in a 1:4 molar ratio in a ball mill for 12 h, and then salt in a 1:1 weight ratio of salt:mixture was added. Ethyl alcohol was then added to form a slurry, followed by another 12 h of ball milling. The obtained slurry was completely dried at 50 °C.
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